An experimental study involving Particle Image Velocimetry (PIV) and far-field microphone measurement was carried out to investigate the mixing characteristics of a low aspect ratio supersonic rectangular nozzle (design Mach number 1.44). Rectangular jets have unique flow characteristics that may make them superior to traditional circular nozzles. Rapid decay of the jet potential core, and enhanced mixing of the ambient fluid with the jet exhaust, can have a significant reduction in the jet noise produced. To determine the radiated sound field from the jet, acoustic measurements were taken in the anechoic chamber of the FCAAP Hot Jet facility, using nine microphones arranged in an arc around the nozzle exit. The experiments were conducted at the ideal operating condition and select conditions above and below ideal. Measurements were taken at both orientations of the rectangular nozzle: major and minor axis. The insulated walls of this Hot Jet facility minimize sound reflections and increase the accuracy of the acoustic measurements. Analysis of the acoustic data revealed a highly directional sound field. The overall sound pressure levels (OASPL) were lower in the major axis as compared to the minor axis. PIV measurements were taken in the FCAAP STOVL facility to reveal the flow pattern at the different operating conditions. PIV is an optical measurement technique that injects very small glycol-based water droplets into the jet stream. A high-speed camera acquires images of the flow field; and special processing software is used to reveal the flow structures present and determine the time-averaged velocity of the jet. Each operating condition produced a unique flow field pattern. At the ideal condition, there was an absence of shock cells and relatively minimal turbulence downstream. At non ideal conditions, shock cells were clearly visible, with increased turbulence downstream. The acoustic levels at the ideal condition were lower than that at the non-ideal conditions. Investigating the relationship between the flow field and the radiated sound field is crucial in helping researchers understand how rectangular nozzles, particularly those of low aspect ratio, can be integrated into the design of newer quieter aircraft, both in the subsonic and supersonic regime.